Category: writing

Monday, 7 May 2012

07:35 – I finished the group on impression analysis yesterday and got started on the group on gunshot and explosive residues analysis. I had intended to include with the kit tiny specimens of firearms propellants (smokeless powder, black powder, Pyrodex) and explosives (dynamite, RDX, PETN, and so on). By “tiny”, I mean specimens of maybe 50 mg. Call it a tenth the size of an aspirin tablet. I was surprised to find that it’s illegal to mail these things. Not just under the Small Quantity Exemption, but period.

Fortunately, I checked the SQE rules. Until now, all of the hazardous materials I’ve been including the kits has fallen under paragraph 334.2(a) or 334.2(b), which qualify up to 30 mL or 30 g of material, respectively, for shipping under SQE. Paragraph 334.2(c) exempts “1 g (0.04 oz) or less for Division 6.1 (Packing Group I) materials”. I wasn’t sure what was included in Class 6 until I looked it up. It turns out to be “Toxic substances and infectious substances”. Alas, explosives (including firearms propellants) are in Class 1, for which there is no SQE (or ORM-D) waiver. That means it’s simply illegal to mail Class 1 materials, no matter how small the quantity. So I’ll have to fall back on telling readers to get their own specimens, which actually isn’t as difficult as it seems at first glance.

Barbara and I have started watching the shortened season three of Crossing Jordan on Netflix streaming. (The actress who plays Jordan was pregnant, which resulted in a season of only 13 episodes.) Fortunately, I happened to notice a post on a forum that mentioned that NBC had run season three not just out of order, but *really* out of order. So, instead of watching the episodes in the order they were broadcast, which is the order that Netflix streaming has them in, we’re watching them in the order they were intended to be broadcast:

1. episode #13
2. episode #7
3. episode #3
4. episode #1
5. episode #12
6. episode #2
7. episode #4
8. episode #9
9. episode #5
10. episode #6
11. episode #11
12. episode #8
13. episode #10


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Sunday, 6 May 2012

08:26 – Barbara is cleaning house this morning and then heading off to her parents’ house for lunch. She’ll make a small Costco run on her way home.

I’m still working on the impression analysis lab sessions. Once I finish this group, all that remains are the groups on gunshot and explosives residues, forgeries and fakes, and forensic biology. Those and the front matter. I’m hoping to finish all of those with several days to spare before the 31 May deadline so that I can go back and do some polishing before submission and maybe even add a lab session or two.

I’ve been issuing purchase orders for materials for the forensic kits as I finish each group of lab sessions, so I’ve already accumulated a lot of stuff. The only exception is the chemical orders, which I’ll combine once I know everything I need to order.


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Saturday, 5 May 2012

08:13 – Barbara spread about 3,058,180 mL of the mulch yesterday, leaving a gigantic 37 mL (2+ tablespoons) pile of the stuff in the driveway. While she was working, we had Colin on a tie-out in the front yard. Someone came down the street walking a dog, and Colin charged out to see them at a dead run. So much for that collar. The plastic quick-release snap connector fractured. We have a drawer full of old collars, and I was going to replace Colin’s collar with a very robust one that used a standard buckle instead of a quick-release plastic snap connector. Barbara pointed out that if Colin had been wearing one of those he might have broken his neck. So we replaced his collar with another snap connector model.

I finished up the bloodstains stuff yesterday and got started on the group of lab sessions on impression analysis. If I have time, I’m going to add a session to that group. Just about every recent cop show has the cops standing around a whiteboard in the squad room, using dry-erase markers to add information to it. Well, it may surprise some people to know that criminals are also big users of whiteboards and dry-erase markers. And, like most people, criminals usually use erasers to erase the stuff on those whiteboards.

But using an eraser on a whiteboard doesn’t actually erase what’s on it. All it does is remove the microscopically thin layer of dried ink powder, leaving traces of the carrier on the board. Those traces can be dusted with fingerprint powder to make them readable. Although I can’t find anything in the literature about using iodine fuming to make those latent traces visible, I suspect that might work at least as well as dusting. I’ll try it. Meanwhile, smart criminals use a paper towel soaked in isopropanol to wet-erase their dry-erase boards. I’ve already tried that, and found that it makes dusting useless to recover latent traces.


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Friday, 4 May 2012

07:27 – I finished the group of lab sessions on revealing latent fingerprints yesterday, and got started on blood. I think we’ll include only one or two sessions on revealing bloodstains. The problem is that, with the exception of Kastle-Meyer reagent, blood reagents are (a) extremely expensive, too much so for a kit, and/or (b) very hazardous, and/or (c) require specialized equipment like a forensic alternate light source, and/or (d) just don’t work very well. Meanwhile, stuff for the forensic science kits is starting to accumulate in large piles.

Barbara is taking a day off work to run errands and get some stuff done around home. She had a pile of mulch dumped in the driveway yesterday. I estimate there’s about 3,058,207 mL of the stuff. Right after the guy left, Colin ran over to the pile, sniffed it, grabbed a mouthful, and ate it.

If you want to grab any O’Reilly ebooks, today’s the day. They’re having a 50% off sale on all titles, and all of them are DRM-free.


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Thursday, 3 May 2012

07:30 – I’m still cranking away on the group of lab sessions on revealing latent fingerprints. Speaking of which, here’s an interesting factoid for Trivial Pursuit: humans and the other great apes are the only creatures that have fingerprints, with one exception. If an Australian cop finds a victim who’s been beaten to death with a eucalyptus club that’s covered in fingerprints, he’d first look for suspects among the local gang of koalas, who are the only creatures other than Hominidae who possess fingerprints. Also, of course, koalas are known for their nasty tempers.


15:10 – I just got this from O’Reilly.

You may have noticed that we’re supporting the FSF’s Day Against DRM. You can read more about it at http://www.fsf.org/news/may-4-day-against-drm. Tomorrow, Friday, 4 May, we are celebrating with a sale in celebration of the Day Against DRM and encouraging customers to try a DRM-free ebook if they haven’t already done so. Here is our messaging:

In Celebration of *Day Against DRM*
Save 50% on ALL Ebooks & Videos

Having the ability to download files at your convenience, store them
on all your devices, or share them with a friend or colleague as you would
a print book, is liberating, and is how it should be. If you haven’t tried
a DRM-free ebook of video, we encourage you to do so now. And if you’re
already a fan, take advantage of our sale and add to your library.

For one day only, you can save 50% on all O’Reilly, No Starch, and Rocky Nook ebooks and videos. Use code: DRMFREE

Ebooks from oreilly.com are DRM-free. You get free lifetime access, multiple file formats, free updates. Deal expires May 4, 2012 at 11:59pm PT and cannot be combined with other offers.

We’ll be extending our sale to include the entire catalog of ebooks and videos from O’Reilly, No Starch, and Rocky Nook — yours included. The deal won’t go live until 12:01 am PT Friday, May 4.

Here’s the tweet we’ll be sending throughout the day, and we’d appreciate anything you can do to get the word out.

RT: @OReillyMedia Celebrate #DayAgainstDRM: Save 50% on all Ebooks & Videos – Use code: DRMFREE http://oreil.ly/Against-DRM Today only!

Feel free to customize it for your ebook or video, and we’d love to have you share it.

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Wednesday, 2 May 2012

09:06 – Thirty days and counting to the deadline on the forensics book. As always, we’ll make the deadline, but we’ll be using every minute available before then to get the book ready to roll.

I finished work on the glass and plastic analysis group of lab sessions yesterday, and I’m well into the group on revealing latent fingerprints. I am going to drop one of the lab sessions that covers developing latent prints with silver nitrate. When I wrote the original draft, silver nitrate was selling for $0.70 to $0.80 per gram. Right now, it’s more like $3.50 to $4.00 per gram, and who knows where it’ll be a year or two from now. Given the amount needed, that’s simply too expensive to include in a kit. It’d be one thing if it was really needed, but silver nitrate development of latent prints is similar enough to other development methods that it’s an easy decision to leave it out.


13:30 – I just ordered 100 grams of ninhydrin crystals for $70. That’s enough ninhydrin to make up 15 to 20 liters of working solution, which is probably a year’s supply for a typical forensics lab, and enough for 150 or more forensics kits.

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Tuesday, 1 May 2012

09:18 – I did go ahead and make up one liter of the 0.1 M IKI solution from solid iodine and potassium iodine. A tenth mole of each in 20 mL of water forms a brown-black sludge that looks like tar. So, with the IKI I already had on hand, I now have enough to make up 40 or so 30 mL bottles. Once the other liter finally goes into solution, I’ll have enough for 30 more.

I almost finished the glass and plastic analysis group of lab sessions for the forensics book yesterday. I’ll finish that today and start on the fingerprinting group. That’s a pretty large group, but I should be able to finish it this week.

Speaking of forensics, Barbara and I recently started watching Crossing Jordan again. We’d already watched the first season, which was released on DVD some years ago. But there was then some issue with music copyrights that for several years made it impossible for the studio to release seasons two through six. In March, all six seasons showed up on Netflix streaming, so we started watching it again where we’d left off.

The cast is good. The writing is generally competent, if not great. Sure, they put their characters in a lot of unrealistic situations, but that’s TV. What’s interesting is how they present forensic science. Unlike Bones, with its imaginary forensics, with minor exceptions Crossing Jordan sticks pretty much to the real deal. Yeah, they sometimes do things that are imaginary in 2012 and would have been really imaginary in 2002, like putting two blood samples into a desktop gene sequencer, punching a button, and four seconds later having Southern blots show up on the computer display, which flashes “DNA MATCH!”. But overall they get the science pretty much right. They also get the personality traits right, particularly with Bug (a forensic entomologist) and Nigel (a forensic technician).

We’re also well into season three of Heartland, which a lot of people think of as the Canadian version of McLeod’s Daughters. We liked the first couple seasons of McLeod’s Daughters, but it quickly went down the tubes after they killed off Claire. As long as Heartland doesn’t make the mistake of killing off Amy, they should be good for a 10 or 15 year run. The cast is first-rate, as is the writing.

Over the years, I’ve rated several hundred series and movies on Netflix, and given fewer than a dozen of those five stars. Heartland gets five stars, at least so far.


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Monday, 30 April 2012

07:35 – We’d be ready to build more chemistry kits, except for one thing. Each kit includes a 30 mL bottle of 0.1 M IKI (iodine/potassium iodide) solution. I’m now waiting for iodine to dissolve.

Iodine is very poorly soluble in water, something like 300 mg/L at room temperature. That changes if iodide ions are present in the water. Molecular iodine–a neutral molecule made up of two iodine atoms–reacts with an iodide ion to form a triodide ion, which is extremely soluble in water. IKI solutions contain iodine and iodide ions in water, with the iodide ions typically in at least small excess. The solution we supply is 0.1 molar with respect to both iodine and iodide, which means there’s no excess iodide. That solution is made up of 12.69 grams of iodine and 16.60 grams of potassium iodide per liter.

The problem is, iodine is tightly controlled by the DEA because it’s used by illegal methamphetamine labs. I do have some on hand, but I try to reserve it for situations where I really need elemental iodine. Accordingly, I’ve been buying an IKI solution from one of my vendors that contains 22 grams of iodine and 40 grams of potassium iodide per liter, then adding iodine crystals to bring it up to equimolar, and then diluting to give an IKI solution that’s 1.26% iodine and 1.66% potassium iodide. But iodine dissolves very, very slowly in that 2.2%/4% solution. By “slowly” I mean a week or two with frequent swirling. So, right now, there’s a one-liter volumetric flask sitting on my lab bench with a few grams of undissolved iodine sitting in the bottom. Fortunately, I already had some of the IKI solution made up, but not enough for 30 kits. So I’ll probably bottle that and make up how ever many kits that IKI solution will cover.

The really annoying thing is that although iodine dissolves very slowly in a dilute KI solution, it dissolves quickly in a concentrated KI solution. If I were making up this solution from scratch, I’d dissolve 16.60 grams of potassium iodide in about 20 mL of distilled water and add 12.69 grams of crystal iodine. The iodine would go into solution within a few minutes.

In fact, I think that’s what I’ll do. The stuff in the volumetric flask, when it finally dissolves, can be used for the next batch of kits. It’s not like anything is going to be growing in a 1.26% solution of iodine. And as to my supply of crystal iodine, I may just do what someone suggested a week or so ago. Order it on eBay. I see that there are several vendors offering ACS Reagent grade iodine crystals in 250 g or 500 g bottles for reasonable prices.


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Sunday, 29 April 2012

08:22 – Barbara got quite a bit done on the chemistry kits yesterday. Today we should finish up the rest of the items we need to assemble 30 more of those. While Barbara works on those, I’ll continue work on the forensic science book.


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Saturday, 28 April 2012

07:58 – Inventory of the chemistry kits is getting critically low, so while I work on the forensics book this weekend Barbara will be working on chemistry kits. We’ll put together another couple dozen of those. I also need to create and issue purchase orders for more components for the chemistry and biology kits, not to mention some initial orders for the forensic science kits.


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